HSCScience Chemistry · Y12 · M7
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Year 12 Chemistry Module 7 · Organic Chemistry ⏱ ~45 min 5 MC · 3 Short Answer Lesson 12 of 23

Reactions of Alcohols — Dehydration, Substitution & Oxidation

Master the three core transformations of alcohols: eliminate water to make alkenes, swap –OH for a halogen, or strip electrons to build aldehydes, ketones and carboxylic acids — and learn exactly which conditions control which product.

Today's hook: A breathalyser turns orange dichromate green when you breathe into it — but why does the same oxidant stay orange when tested on a tertiary alcohol?
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Worksheets

Practise this lesson

Four printable worksheets that build from the foundations up to exam-style questions — start at whatever level suits you.

Before You Read

Three Industries, One Molecule

A forensic breathalyser works by oxidising ethanol in breath to ethanoic acid using potassium dichromate — the orange dichromate turns green as it is reduced. A winemaker monitors the souring of wine into vinegar (ethanol → ethanoic acid) when wine is exposed to air. A polymer chemist dehydrates ethanol to ethene, which is then polymerised to polyethylene.

Before you read on: Write down what you think is the structural difference between the product of oxidation (ethanoic acid, CH₃COOH) and the product of dehydration (ethene, CH₂=CH₂). What bonds have been added to, or removed from, the ethanol molecule in each case?

Learning Intentions
By the end of this lesson you will:

Know

  • Three reactions of alcohols: dehydration, substitution with HX, oxidation
  • Oxidation outcomes: 1° → aldehyde (distillation) or COOH (reflux) · 2° → ketone · 3° → no reaction
  • Colour changes: K₂Cr₂O₇/H⁺ orange→green (oxidation occurred) or stays orange (no oxidation)
  • HX reactivity order: HI > HBr > HCl

Understand

  • Why tertiary alcohols cannot be oxidised — no H on C–OH carbon
  • Why distillation gives aldehyde but reflux gives carboxylic acid from the same primary alcohol
  • Why concentrated (not dilute) acid drives dehydration
  • Why H₂O is always a product of alcohol substitution with HX

Can Do

  • Write balanced equations for all three reaction types with correct conditions
  • Classify an unknown alcohol as 1°/2°/3° from oxidation test results
  • Select conditions to produce a specific oxidation product from a primary alcohol
  • Construct multi-step synthesis routes using alcohols as intermediates
Scan these before reading
Key Terms
DehydrationAn elimination reaction removing H₂O from an alcohol to form an alkene; requires H₂SO₄ catalyst at ~170°C.
Nucleophilic substitutionReaction of an alcohol with HX to replace –OH with a halogen; produces a halogenoalkane.
Oxidation of primary alcoholPrimary alcohols oxidise to aldehydes (gentle oxidant) and then to carboxylic acids (excess oxidant).
Oxidation of secondary alcoholSecondary alcohols oxidise to ketones; no further oxidation under normal conditions.
Tertiary alcohol oxidationTertiary alcohols resist oxidation because there is no C–H bond adjacent to the –OH group.
Acidified dichromate testK₂Cr₂O₇/H₂SO₄ changes from orange to green in the presence of oxidisable alcohols (primary or secondary).
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Dehydration of Alcohols — Making Alkenes

Dehydration is the exact reverse of hydration — water is eliminated across the C–OH bond and an adjacent C–H bond, regenerating the C=C double bond — and the conditions that drive this reversal are the opposite of those that drive hydration.

Dehydration is an elimination reaction in which an alcohol loses a water molecule (H from one carbon, OH from the adjacent carbon) to form an alkene. It is the reverse of alkene hydration (L06, L10).

R–CH₂–CH₂OH → R–CH=CH₂ + H₂O

Worked Equations

Ethanol → ethene:
CH₃CH₂OH → CH₂=CH₂ + H₂O
Conditions: conc. H₂SO₄, ~170°C

Propan-1-ol → propene:
CH₃CH₂CH₂OH → CH₃CH=CH₂ + H₂O
Conditions: conc. H₂SO₄ or conc. H₃PO₄, heat

Secondary and Tertiary Alcohols — Two Possible Products

When a secondary or tertiary alcohol is dehydrated, the H can be removed from either adjacent carbon, giving two possible alkene products. The major product is the more substituted alkene (more alkyl groups on the C=C carbons). For HSC, NESA accepts any alkene product, but the more substituted alkene is preferred.

Butan-2-ol dehydration:

CH₃CHOHCH₂CH₃ → CH₃CH=CHCH₃ + H₂O  (but-2-ene — major, more substituted)
CH₃CHOHCH₂CH₃ → CH₂=CHCH₂CH₃ + H₂O  (but-1-ene — minor, less substituted)

butan-2-ol (reactant) CH₃ C H OH C H H CH₃ OH + H → H₂O (eliminated) conc. H₂SO₄ heat but-2-ene (major product) CH₃ CH CH CH₃ + H₂O C=C

Dehydration of butan-2-ol — H removed from C3 and OH removed from C2 combine to form H₂O; C=C forms between C2 and C3 giving but-2-ene (major, more substituted product)

Hydration vs. Dehydration — Opposite Conditions

HYDRATION (alkene → alcohol)
dilute acid · high P · high T
adds H₂O across C=C
DEHYDRATION (alcohol → alkene)
conc. acid · atmospheric P · heat
removes H₂O from C–OH and adjacent C–H
Conditions — Dehydration:
Reagent: conc. H₂SO₄ or conc. H₃PO₄ (acid catalyst + dehydrating agent)
Temperature: ~170°C for ethanol; ~230°C+ for higher alcohols
Pressure: Atmospheric
Equipment: Distillation (the product is allowed to evaporate from the heated mixture and is collected separately, used when the product needs to be removed as it forms) — removes volatile alkene product as formed
Must Do: The acid in dehydration is CONCENTRATED — not dilute. Dilute acid + high pressure drives hydration (the reverse reaction). Writing "dilute H₂SO₄" for dehydration is wrong — concentrated acid at higher temperature drives dehydration. The concentration of the acid determines the reaction direction.
Common Error: Writing "water is added in dehydration." This is the exact opposite. DEhydration means removing water (–de = removal, hydration = water). The –OH from the alcohol and an H from the adjacent carbon leave together as H₂O — the molecule gets smaller. If water appears as a reactant in your dehydration equation, you have written a hydration reaction instead.
Quick check: Which acid and conditions are needed for dehydration of an alcohol?
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Substitution of Alcohols with HX — Making Haloalkanes

The reverse of the haloalkane substitution from L10 — instead of converting a haloalkane to an alcohol with NaOH, you can convert an alcohol to a haloalkane with HX — and the conditions and halide reactivity order are what HSC specifically tests.

When an alcohol is treated with a hydrogen halide (HX), the –OH group is replaced by the halogen, producing a haloalkane and water:

R–OH + HX → R–X + H₂O

Halide Reactivity Order

HI
fastest
C–I easiest to form
>
HBr
intermediate
>
HCl
slowest
C–Cl hardest to form

Worked Equations:

CH₃CH₂OH + HBr → CH₃CH₂Br + H₂O  (bromoethane)
CH₃CH₂CH₂OH + HI → CH₃CH₂CH₂I + H₂O  (1-iodopropane)

Comparison — reverse reactions:

R–OH + HX → R–X + H₂O  (alcohol → haloalkane — this lesson)
R–X + NaOH(aq) → R–OH + NaX  (haloalkane → alcohol — L10)

Conditions — Substitution of Alcohol with HX:
Reagent: HCl, HBr, or HI (gas or concentrated aqueous solution)
Catalyst: None (ZnCl₂ sometimes used with HCl for primary alcohols)
Conditions: Heat under reflux (the reaction mixture is heated with a condenser returning vapour to the flask, allowing the reaction to proceed at high temperature without losing volatile reactants or products)
Equipment: Reflux condenser; fume cupboard (HX gases are corrosive)
Must Do: Always include H₂O as a product. R–OH + HBr → R–Br is incomplete — the equation is unbalanced without H₂O. Check: the –OH from the alcohol and the H from HX combine on the right side to give H₂O. Missing H₂O is one of the most commonly penalised equation errors.
Common Error: Confusing R–OH + HX → R–X + H₂O (alcohol substitution) with alkene + HX → haloalkane (hydrohalogenation from L06, addition). Both use HX and produce haloalkanes. Key differences: (1) starting material (alcohol vs alkene); (2) whether H₂O is also produced (yes for alcohol substitution; no for addition); (3) reaction type (substitution vs addition). The presence of H₂O as a product instantly identifies alcohol substitution.
True or False: When ethanol reacts with HBr, water is produced as a co-product.
3

Oxidation of Alcohols — The Classification-Dependent Reaction

Oxidation of alcohols is the single most important reaction for understanding how the organic functional group classes connect — primary alcohols become aldehydes and then carboxylic acids, secondary alcohols become ketones, and tertiary alcohols refuse to react — and the reason is structural, not arbitrary.

Why Oxidation Depends on Alcohol Classification

Oxidation of an alcohol involves removing two hydrogen atoms — one H from the C–OH carbon and one H from the –OH oxygen — to form the C=O (carbonyl) bond. For this to be possible, the C–OH carbon must have at least one H atom available to be removed.

C–OH has 2 H atoms → gives aldehyde (distillation) → can further oxidise to carboxylic acid (reflux)
C–OH has 1 H atom → gives ketone. Ketone C=O is flanked by two carbons — no H on carbonyl carbon → cannot be further oxidised
C–OH has 0 H atoms (bonded to 3 carbons) → no H to remove → NO REACTION with K₂Cr₂O₇/H⁺

Controlling Product from Primary Alcohols — Distillation vs. Reflux

Distillation → Aldehyde

Aldehyde has lower BP than alcohol — collected as it forms before excess oxidant can oxidise it further. Removes product from reaction mixture immediately.

R–CH₂OH + [O] → R–CHO + H₂O
Reflux → Carboxylic Acid

All components stay in flask; excess oxidant has maximum contact time to fully oxidise aldehyde intermediate through to carboxylic acid.

R–CH₂OH + 2[O] → R–COOH + H₂O

Oxidation Summary Table

Alcohol Class Oxidant Equipment Product Colour Change
Primary (1°)K₂Cr₂O₇/H⁺DistillationAldehydeOrange → Green
Primary (1°)K₂Cr₂O₇/H⁺ (excess)RefluxCarboxylic acidOrange → Green
Secondary (2°)K₂Cr₂O₇/H⁺RefluxKetoneOrange → Green
Tertiary (3°)K₂Cr₂O₇/H⁺AnyNo reactionStays orange
Must Do — Two Conditions Required: For any alcohol oxidation answer, always state: (1) the oxidising agent (K₂Cr₂O₇/H⁺ — always acidified); AND (2) the equipment (distillation for aldehyde; reflux for carboxylic acid or ketone). Stating only the reagent without the equipment earns partial marks. The equipment choice determines the product.
Common Error: "Tertiary alcohols give a ketone with KMnO₄." Tertiary alcohols do NOT undergo oxidation — the solution stays orange. This is the diagnostic test for tertiary alcohols.
Common Error: "KMnO₄ goes purple → orange." KMnO₄ goes purple → colourless (Mn²⁺) in acidic solution. Orange is the colour of dichromate. KMnO₄ NEVER turns orange.
A student oxidises butan-2-ol with K₂Cr₂O₇/H₂SO₄ under reflux. What is the product and colour change?
4

Alcohols at the Centre — The Reaction Map Hub

Putting dehydration, substitution, and oxidation together with the production reactions from L10 reveals that alcohols are the central hub of the organic reaction map — every arrow into and out of alcohol connects to a different functional group class.

ALCOHOL R–OH ALKENE hydration (L10) HALOALKANE NaOH(aq) (L10) GLUCOSE fermentation (L10) ALKENE conc. H₂SO₄, heat dehydration HALOALKANE + HX, reflux ALDEHYDE (1° only) K₂Cr₂O₇/H⁺ distillation · 1° CARBOXYLIC ACID (1° only) excess K₂Cr₂O₇/H⁺ reflux · 1° KETONE (2° only) K₂Cr₂O₇/H⁺ reflux · 2° NO REACTION (3° stays orange) ARROWS IN (production) ARROWS OUT (this lesson)

Alcohol reaction hub — dashed arrows show production routes (L10); solid arrows show this lesson's reactions. Alcohol is the central node connecting every major functional group class.

Must Do: The orange→green colour change confirms oxidation occurred — it does NOT identify the specific product. To determine the product, you need: (1) the conditions (distillation vs. reflux); AND (2) a secondary test on the product (Tollens' for aldehyde vs. litmus for acid). Never write "the product is an aldehyde because the dichromate went green" — the colour change identifies the class (primary/secondary) but not the specific carbonyl product.
Complete: To convert a primary alcohol to a carboxylic acid, use _____ oxidant under _____ conditions (equipment).
WE
Predicting Products of Alcohol Reactions

Problem: For each reaction below, write the balanced equation, name the product, and state all conditions: (a) dehydration of propan-1-ol; (b) reaction of butan-1-ol with HBr; (c) oxidation of propan-2-ol to its maximum oxidation product.

1
(a) Dehydration of propan-1-ol:
Propan-1-ol: CH₃CH₂CH₂OH. Remove H from C2 and –OH from C1 → propene + H₂O.
CH₃CH₂CH₂OH → CH₃CH=CH₂ + H₂O
Product: propene | Conditions: conc. H₂SO₄ (or conc. H₃PO₄) · heat (~170–230°C) · distillation
2
(b) Butan-1-ol + HBr:
CH₃CH₂CH₂CH₂OH + HBr → CH₃CH₂CH₂CH₂Br + H₂O
Product: 1-bromobutane | Conditions: HBr · heat under reflux · fume cupboard
3
(c) Oxidation of propan-2-ol (maximum product):
Propan-2-ol: CH₃CHOHCH₃ — secondary alcohol. Maximum oxidation product = ketone. Ketones cannot be further oxidised.
CH₃CHOHCH₃ + [O] → CH₃COCH₃ + H₂O
Product: propanone | Conditions: K₂Cr₂O₇/H₂SO₄ · reflux · Colour change: orange → green
Summary:
(a) CH₃CH₂CH₂OH → CH₃CH=CH₂ + H₂O (propene). Conc. H₂SO₄, heat, distillation.
(b) CH₃CH₂CH₂CH₂OH + HBr → CH₃CH₂CH₂CH₂Br + H₂O (1-bromobutane). HBr, reflux.
(c) CH₃CHOHCH₃ + [O] → CH₃COCH₃ + H₂O (propanone). K₂Cr₂O₇/H₂SO₄, reflux. Orange → green.
WE
Identifying Unknown Alcohols Using Oxidation Tests

Problem: Three unlabelled alcohols — P, Q, R — all have molecular formula C₄H₁₀O. When treated with acidified K₂Cr₂O₇: P stays orange. Q turns green; distillation of the product gives a compound that produces a silver mirror with Tollens' reagent. R turns green; the product does NOT give a silver mirror and does NOT turn litmus red. (a) Classify P, Q, R as 1°/2°/3°. (b) Identify each compound. (c) Write the oxidation equation for Q under reflux conditions.

1
(a) Classify:
P: no colour change → no oxidation → tertiary alcohol
Q: orange → green; positive Tollens' → aldehyde formed → primary alcohol
R: orange → green; neither aldehyde nor carboxylic acid → ketone formed → secondary alcohol
2
(b) Identify (all C₄H₁₀O isomers):
P (tertiary, C₄): only one tertiary C₄ alcohol → 2-methylpropan-2-ol ((CH₃)₃COH)
Q (primary, C₄): most common exam assumption → butan-1-ol (CH₃CH₂CH₂CH₂OH)
R (secondary, C₄): only one secondary C₄H₁₀O alcohol → butan-2-ol (CH₃CHOHCH₂CH₃)
3
(c) Oxidation of Q (butan-1-ol) under reflux — maximum product:
Primary alcohol + excess oxidant + reflux → carboxylic acid.
CH₃CH₂CH₂CH₂OH + 2[O] → CH₃CH₂CH₂COOH + H₂O
Product: butanoic acid. Conditions: excess K₂Cr₂O₇/H₂SO₄, reflux. Orange → green.
Key Equations — Reactions of Alcohols
Dehydration (Elimination)
R–CH₂–CH₂OH → R–CH=CH₂ + H₂O
conc. H₂SO₄ or conc. H₃PO₄ · heat (~170°C) · atmospheric pressure
Substitution with HX
R–OH + HX → R–X + H₂O
HCl, HBr, or HI · heat under reflux · reactivity: HI > HBr > HCl
Oxidation: 1° → Aldehyde
R–CH₂OH + [O] → R–CHO + H₂O
K₂Cr₂O₇/H⁺ · distillation · orange → green
Oxidation: 1° → Carboxylic Acid
R–CH₂OH + 2[O] → R–COOH + H₂O
excess K₂Cr₂O₇/H⁺ · reflux · orange → green
Oxidation: 2° → Ketone
R–CHOH–R' + [O] → R–CO–R' + H₂O
K₂Cr₂O₇/H⁺ · reflux · orange → green · cannot oxidise further
Tertiary → No Reaction
R–C(OH)(R')(R'') + [O] → no reaction
K₂Cr₂O₇/H⁺ stays ORANGE · no H on C–OH carbon
Interactive Tool — Alcohols Laboratory Open fullscreen ↗
In the Alcohol Properties tool, which type of alcohol CANNOT be oxidised to a carboxylic acid?
🔀 Sort the Steps +7 XP
Arrange the correct sequence of steps to oxidise ethanol all the way to ethanoic acid using acidified K₂Cr₂O₇:
Mix ethanol with acidified potassium dichromate (K₂Cr₂O₇/H₂SO₄)
Heat under reflux conditions (not distillation) to prevent loss of intermediate
Ethanol (primary alcohol) is first oxidised to ethanal (aldehyde)
Continued oxidation converts ethanal to ethanoic acid (carboxylic acid)
Observe colour change from orange (Cr₂O₇²⁻) to green (Cr³⁺) confirming oxidation

Complete the Learn phase to unlock Practice.

Activity A — Conditions Grid: Fill the Gaps

For each transformation below, write: the reagent, the conditions (temperature/equipment), and the type of reaction.

  1. Butan-1-ol → but-1-ene
  2. Pentan-1-ol → pentanal
  3. Pentan-1-ol → pentanoic acid
  4. Propan-2-ol → propanone
  5. Ethanol + HCl → chloroethane

Activity B — Diagnostic Reasoning: What Alcohol Is This?

An unknown alcohol X (molecular formula C₃H₈O) is tested with the following reagents:

  • K₂Cr₂O₇/H₂SO₄ (reflux): solution turns green; product has a sharp vinegar-like smell
  • Dehydration with conc. H₂SO₄: produces propene

Identify alcohol X, write its structural formula, and explain each piece of evidence. Then write the equation for the oxidation of X to its maximum oxidation product.

Q1. A student adds excess acidified K₂Cr₂O₇ to pentan-1-ol under reflux. What is the organic product and what colour change is observed?

Q2. Which conditions would convert ethanol to ethanal (acetaldehyde) rather than to ethanoic acid?

Q3. A student treats 2-methylpropan-2-ol with acidified K₂Cr₂O₇. What does the student observe, and why?

Q4. Which conditions would correctly convert butan-1-ol to butanal (and NOT butanoic acid)?

Q5. A compound with molecular formula C₄H₈O does not give a positive Tollens' test and does not react with acidified K₂Cr₂O₇ (solution stays orange). What is the most likely identity of this compound?

Q6 — Short Answer (4 marks)

Write balanced equations for three reactions of ethanol: (a) dehydration to ethene; (b) reaction with HBr to form a haloalkane; (c) oxidation to ethanoic acid. For each equation, state the reagents and conditions required.

Q7 — Short Answer (5 marks)

The same primary alcohol — pentan-1-ol — can be converted to either pentanal or pentanoic acid using K₂Cr₂O₇/H₂SO₄. (a) Write the equation for each transformation. (b) State the specific conditions (including equipment) that produce each product. (c) Explain why using reflux rather than distillation changes the product from aldehyde to carboxylic acid.

Q8 — Short Answer (6 marks)

A student performs a two-step synthesis: Step 1 — ethene is reacted with steam to produce ethanol. Step 2 — ethanol is converted to ethanoic acid. For each step, write the balanced equation, state the reagents and conditions, and explain the role of a specific condition in determining the product (including why reflux in step 2 gives acid rather than aldehyde).

Show All Answers

Multiple Choice Answers

Q1 — B: Pentan-1-ol is a primary alcohol. Excess K₂Cr₂O₇/H⁺ under REFLUX gives carboxylic acid (pentanoic acid). Orange → green. A would result from DISTILLATION. C is wrong — pentan-1-one would require a secondary alcohol. D has wrong colour change — purple→colourless is KMnO₄.

Q2 — B: To produce the aldehyde from a primary alcohol, the aldehyde must be removed before excess oxidant can oxidise it further — achieved by DISTILLATION. A (excess oxidant, reflux) fully oxidises to ethanoic acid. D describes dehydration to ethene — not oxidation.

Q3 — C: 2-methylpropan-2-ol is a tertiary alcohol — the C–OH carbon is bonded to three other carbons with no H atoms. K₂Cr₂O₇/H⁺ stays orange = no oxidation. This orange/no-change result is the diagnostic test for tertiary alcohols.

Q4 — C: To stop at the aldehyde stage, the aldehyde must be removed from the reaction mixture as soon as it forms — before the oxidant can oxidise it further to butanoic acid. Distillation achieves this because butanal has a lower boiling point than butan-1-ol.

Q5 — D: No reaction with K₂Cr₂O₇/H⁺ (stays orange) → not a primary or secondary alcohol and not an aldehyde. No positive Tollens' → not an aldehyde. C₄H₈O with a C=O that is not an aldehyde = ketone. Butan-2-one (CH₃COCH₂CH₃) is the C₄ ketone.

Short Answer Sample Answers

Q6 (4 marks): (a) CH₃CH₂OH → CH₂=CH₂ + H₂O. Conditions: conc. H₂SO₄, heat (~170°C), distillation. (b) CH₃CH₂OH + HBr → CH₃CH₂Br + H₂O. Conditions: HBr, heat under reflux. (c) CH₃CH₂OH + 2[O] → CH₃COOH + H₂O. Conditions: excess K₂Cr₂O₇/H₂SO₄, reflux.

Q7 (5 marks): (a) Pentanal: CH₃CH₂CH₂CH₂CH₂OH + [O] → CH₃CH₂CH₂CH₂CHO + H₂O. Pentanoic acid: + 2[O] → CH₃CH₂CH₂CH₂COOH + H₂O. (b) Pentanal: K₂Cr₂O₇/H₂SO₄, gentle heating, DISTILLATION. Pentanoic acid: excess K₂Cr₂O₇/H₂SO₄, REFLUX. (c) Pentanal has a lower boiling point than pentan-1-ol. Under distillation, pentanal boils off and is removed from the reaction mixture as soon as it forms — before excess oxidant can oxidise it further. Under reflux, all volatile components are condensed and returned to the flask, giving the oxidant maximum contact time to oxidise the aldehyde all the way to the carboxylic acid.

Q8 (6 marks): Step 1: CH₂=CH₂ + H₂O ⇌ CH₃CH₂OH. Conditions: H₂O (steam), H₃PO₄ catalyst, ~300°C, ~65 atm. High pressure used because the left side has 2 moles of gas — by Le Chatelier, high pressure shifts equilibrium right toward ethanol. Step 2: CH₃CH₂OH + 2[O] → CH₃COOH + H₂O. Conditions: excess K₂Cr₂O₇/H₂SO₄, reflux. Role of reflux: keeps all volatile components (including the aldehyde intermediate, ethanal) in the reaction flask, giving the excess oxidant maximum contact time to oxidise ethanal through to ethanoic acid. If distillation were used instead, ethanal would be removed before further oxidation.

How did your thinking change?

Return to your prediction about the structural difference between ethanoic acid (oxidation) and ethene (dehydration), both starting from ethanol. Oxidation: two H atoms removed, C=O and OH group added — functional group changes from –OH to –COOH. Dehydration: –OH and an H from adjacent carbon leave as H₂O, C=C double bond forms. How well did your structural prediction compare?

Coming up in Lesson 13: The oxidation products of primary alcohols (aldehydes) and secondary alcohols (ketones) become the focus — understanding their distinct structural properties, reactivity with Tollens' and Fehling's reagents, and how to distinguish between them experimentally.

What reagent and equipment convert a primary alcohol to an aldehyde (stopping before carboxylic acid)?

Why do tertiary alcohols not react with K₂Cr₂O₇/H⁺?

Give the HX reactivity order and explain why HI is the fastest.

What acid concentration is required for dehydration and why does concentration matter?

A student observes that KMnO₄ turns orange when oxidising an alcohol. What is wrong with this observation?

← Lesson 11 Lesson 13 →
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