Chemistry • Year 11 • Module 4 • Lesson 8

Hess's Law

Synthesise and evaluate — two extended-response questions requiring sustained multi-criteria reasoning, evidence-based judgement, and real-world connections.

Master • Band 5–6 Extended Response

Question 1 — Evaluating energy efficiency in industrial SO₃ production

8 marks

Scenario. A chemical plant produces SO₃ for sulfuric acid manufacture (Contact Process). The plant manager proposes two routes:

Route A (one-step): S(s) + ¾O₂(g) → SO₃(g)

Route B (two-step): Step 1: S(s) + O₂(g) → SO₂(g);   Step 2: SO₂(g) + ½O₂(g) → SO₃(g)

The thermochemical data available are:

EquationΔH (kJ mol⁻¹)
S(s) + O₂(g) → SO₂(g)−297
2SO₂(g) + O₂(g) → 2SO₃(g)−198
S(s) + ¾O₂(g) → SO₃(g)−396

The plant’s energy recovery system can only recapture heat released in the first step of a multi-step route, not from intermediate-step reactions. Assume all reactions go to completion.

Enthalpy S(s) + ¾O₂(g) SO₂(g) + ½O₂(g) SO₃(g) Route A −396 ΔH₁=−297 ΔH₂=−99
Figure 1.1. Enthalpy level diagram comparing Route A (direct, dashed teal arrow) and Route B (two steps, orange and blue arrows) for SO₃ formation. Adapted from standard thermochemical data.

Question. Evaluate whether the plant manager’s choice of route affects the total enthalpy change for the production of SO₃, and assess which route is more useful for the plant’s energy recovery system.

In your response you must:

  1. State and explain Hess’s Law as it applies to both routes (ΔH of Route A vs total ΔH of Route B).
  2. Calculate ΔH for Step 2 of Route B using the data provided; show your working.
  3. Evaluate on at least two criteria (total energy released; energy available in Step 1 alone) which route is more practical for the energy recovery system described.
  4. Identify one limitation of assuming the reactions “go to completion” in an industrial context.
Band 5–6 tip: state Hess’s Law → calculate ΔH(Step 2) using Hess’s Law → compare routes → evaluate → limitation. Do not skip the “evaluate on criteria” step.

Question 2 — Methane formation and the limits of Hess’s Law in practice

8 marks

Scenario. The standard enthalpy of formation of methane, CH₄(g), cannot be measured directly because the reaction C(s) + 2H₂(g) → CH₄(g) does not proceed at measurable rate under standard conditions. A researcher uses Hess’s Law with three combustion enthalpies:

EquationΔH (kJ mol⁻¹)
(1) C(s) + O₂(g) → CO₂(g)−393.5
(2) H₂(g) + ½O₂(g) → H₂O(l)−285.8
(3) CH₄(g) + 2O₂(g) → CO₂(g) + 2H₂O(l)−890.3

The researcher's lab notebook shows the following working — which contains one deliberate error:

Step 1: Reverse (3): CO₂ + 2H₂O → CH₄ + 2O₂   ΔH = +890.3
Step 2: Use (1): C + O₂ → CO₂   ΔH = −393.5
Step 3: Use (2) × 2: 2H₂ + O₂ → 2H₂O   ΔH = −285.8
Step 4: Sum: ΔH = 890.3 + (−393.5) + (−285.8) = +210.8 kJ mol⁻¹

The accepted value is ΔHₑf[CH₄(g)] = −74.8 kJ mol⁻¹.

Question. Identify and explain the error in the researcher’s working, then provide a complete corrected calculation. Evaluate the reliability of Hess’s Law as a method for determining enthalpy values that cannot be measured directly.

In your response you must:

  1. Identify the specific step where the error occurs and state precisely what rule was violated.
  2. Provide the corrected calculation, showing all steps and the correct ΔH.
  3. Verify your answer matches the accepted value and explain what this confirms about Hess’s Law.
  4. Evaluate two reasons why Hess’s Law results from combustion data may still carry small uncertainties in practice, even when the algebra is correct.
Band 5–6 tip: identify the error first (scaling (2) by 2 was not applied to ΔH) → correct working → verify → discuss two practical uncertainties (e.g. impure samples, incomplete combustion in calorimeter, heat loss).
Answers & Marking Guidance — Do not peek before attempting

Q1 — Industrial SO₃ production (8 marks)

1 — Hess’s Law applied: Hess’s Law states that ΔH for a reaction is independent of the pathway taken; enthalpy is a state function. Route A converts S + ¾O₂ → SO₃ in one step (ΔH = −396 kJ mol⁻¹). Route B covers the same conversion in two steps. By Hess’s Law, ΔH(total, B) = ΔH(Step 1) + ΔH(Step 2) = ΔH(Route A) = −396 kJ mol⁻¹. [2 marks: 1 for stating Hess’s Law correctly; 1 for correctly equating total ΔH across both routes]

2 — Calculate ΔH(Step 2): ΔH(Step 2) = total ΔH − ΔH(Step 1) = −396 − (−297) = −99 kJ mol⁻¹. (Equivalently: ½ × (−198) = −99 kJ mol⁻¹ from the given equation scaled by ½.) [1 mark for correct value with working]

3 — Evaluate routes on two criteria:
Total energy released: Both routes release −396 kJ mol⁻¹ total — identical by Hess’s Law. Neither is superior on this criterion. [1 mark]
Energy available in Step 1 for recovery: Route B Step 1 releases −297 kJ mol⁻¹ in a single measurable combustion event (S + O₂ → SO₂) — a larger, easily recoverable heat release. Route A releases all energy in one step too (−396 kJ mol⁻¹). However, Route B’s Step 1 is the most exothermic stage; Step 2 releases only −99 kJ mol⁻¹ and is catalysis-dependent (requires V₂O₅ catalyst at 450°C in practice). If the energy recovery system captures only Step 1 heat, Route B captures −297 kJ mol⁻¹ from Step 1 (76% of total) while Route A captures the full −396 kJ mol⁻¹ in its single step. On balance, Route A is simpler for recovery (one heat exchange point), but Route B may be industrially preferred because SO₂ is an intermediate that can be stored and converted separately under optimised conditions. [2 marks: 1 per criterion evaluated with reference to data]

4 — Limitation: In practice, reactions rarely go to 100% completion — SO₂/SO₃ equilibrium (the Contact Process) typically achieves ~98% conversion at best. Assuming complete conversion overestimates the heat released and the yield of SO₃; actual industrial performance requires correction for equilibrium conversion. [1 mark]

Marking note: award 1 additional quality mark for a response that integrates all four requirements into a coherent, structured argument rather than listing isolated points.

Q2 — Methane formation and error analysis (8 marks)

1 — Identify error: The error is in Step 3. Equation (2) was correctly scaled by 2 (giving 2H₂ + O₂ → 2H₂O), but ΔH was NOT scaled: the student used −285.8 instead of 2 × (−285.8) = −571.6 kJ mol⁻¹. This violates the manipulation rule: any operation applied to the equation must also be applied to ΔH. [2 marks: 1 for identifying Step 3 as the error; 1 for naming the violated rule precisely]

2 — Corrected calculation:
Reverse (3): CO₂ + 2H₂O → CH₄ + 2O₂   ΔH = +890.3 [1]
Use (1) as written: C + O₂ → CO₂   ΔH = −393.5 [1]
Scale (2) × 2: 2H₂ + O₂ → 2H₂O   ΔH = 2(−285.8) = −571.6 [1]
Add all: cancel CO₂, 2H₂O, 2O₂ ✓. Net: C + 2H₂ → CH₄.
ΔH = +890.3 + (−393.5) + (−571.6) = +890.3 − 965.1 = −74.8 kJ mol⁻¹ [1]

3 — Verify and confirm Hess’s Law: The corrected answer (−74.8 kJ mol⁻¹) matches the accepted value exactly. This confirms that Hess’s Law gives a reliable, reproducible ΔH for the target reaction regardless of whether it can be measured directly, as long as the manipulation rules are applied correctly and the given ΔH values are accurate. [1 mark]

4 — Two practical uncertainties:
(a) Calorimeter heat loss: not all heat produced in the combustion is captured in the calorimeter solution — some escapes to the surroundings. This makes the measured ΔH slightly less negative than the true value, introducing systematic error into each component equation. [½ mark]
(b) Purity of samples: if the carbon sample contains impurities (e.g. moisture, non-carbon ash), the mass used in calculations overestimates the number of moles of C combusted, leading to an underestimated magnitude of ΔH per mole. Impure CH₄ similarly introduces error into combustion enthalpy (3). [½ mark]
Accept any two of: heat loss, impure samples, incomplete combustion (CO in products), uncertainty in mass measurement, phase of water product assumed to be liquid. [1 mark total for two valid points]